Verifying manufacturer precision claims Bringing a new analyser or reagent system into service does not mean re-establishing its precision from scratch. CLSI EP15-A3 lets you verify the manufacturer’s claim with a short study. Here is how, and what to do when it fails.

When a clinical laboratory brings a new measurement procedure into service, it has to show the method performs acceptably in its own laboratory. The laboratory does not have to re-derive the manufacturer’s performance characteristics from first principles, because that work was done during development. What the laboratory needs is verification: confirmation that the claimed precision and trueness hold up on its instruments, its operators, its environment. CLSI EP15-A3 is the protocol for exactly that. EP15-A3 is a fraction of the work of a full establishment study.

Establish versus verify: EP05 and EP15

The distinction matters most here, because this is where laboratories most often do more work than they need to. Establishing precision, characterising it from scratch across a full nested design of days, runs, and operators, is EP05-A3. Establishing precision is the manufacturer’s job. Verifying precision, confirming a stated claim holds, is EP15-A3. Verifying it is yours.

EP05-A3 (establish) EP15-A3 (verify)
Who Manufacturer / developer User laboratory
Purpose Characterise precision from scratch Confirm the claim holds in your own laboratory
Typical design ~20 days, nested runs and replicates 5 days × 5 replicates (per EP15-A3)
Output Repeatability through to reproducibility components Repeatability and within-laboratory precision, against the claim
Decision Observed imprecision within the verification limit?

Reaching for EP05 when EP15 would do, running a twenty-day establishment study to bring a well-characterised assay online, is a lot of effort spent confirming what the manufacturer already documented. Verify unless you have a specific reason to establish.

The deciding factor is modification. A cleared assay run exactly as the instructions specify already has established precision claims, so you verify them. Change something about how you use it and those claims no longer describe what you are doing, so you must establish precision yourself.

Your method is… You…
FDA-cleared or CE-marked, used exactly as the instructions specify Verify (EP15-A3)
Laboratory-developed, modified from its cleared use, or used off-label Establish (EP05-A3)

Changing the specimen type, the platform, the dilution or the intended use all count as modification. When you are unsure whether a change counts, treat it as one. Establishing unnecessarily costs you effort, but verifying a method that needed establishing leaves a performance gap you never measured. The same distinction runs more broadly through validation versus verification.

The verification experiment

EP15-A3 folds precision and trueness verification into a single short study. The design is compact: five replicates of each sample per day, over five days, at two or more concentrations spanning the measuring interval. Twenty-five measurements per level, in other words. From that data you estimate two precision components: repeatability (within-run, the scatter of replicates measured close together) and within-laboratory precision, also called intermediate precision (the total day-to-day variation your laboratory will see). Those are the two numbers the manufacturer’s claim is stated against, so those are the two you verify.

The two are often confused, and the difference decides which number you quote. Repeatability covers replicates measured under conditions held as constant as possible: one run, one operator, one calibration, close together in time. Intermediate precision adds the variation that accumulates between runs and between days — recalibration, a fresh reagent vial, a different operator, ordinary environmental drift. Repeatability is always the smaller of the two, and quoting it as the method’s precision understates what a laboratory sees day to day. Intermediate precision is the figure that describes a reported patient result. See the precision components for the full hierarchy and the arithmetic that combines them.

Screen for outliers first. A generalised ESD test identifies aberrant replicates that would otherwise inflate your estimates. A single fumbled measurement can fail an otherwise sound verification.

Precision study plot showing replicate measurements grouped by day across the five-day verification experiment.
A precision and trueness verification study (CLSI EP15-A3, Example 1 — ferritin), from which repeatability and within-laboratory precision are estimated and tested against the manufacturer’s claim.

Comparing against the claim

Verification is a one-sided question: is your observed imprecision consistent with the claim, or meaningfully worse than it? Your estimate comes from a small sample, so it carries real uncertainty. An observed SD slightly above the claimed value does not automatically mean the claim is broken.

EP15-A3 handles this with an upper verification limit. The limit is a threshold derived from the claimed SD and the degrees of freedom in your study, using the χ² distribution, that your observed SD would have to exceed before the exceedance is more than sampling noise.

If your observed imprecision falls at or below the limit, the claim is verified. If it exceeds the limit, the difference is unlikely to be chance and the claim is not verified in your laboratory. This is the correct statistical treatment of “is my SD close enough to theirs?” It accounts for a five-day study being unable to pin down an SD precisely.

Verifying trueness at the same time

EP15-A3 also covers trueness: systematic bias against an assigned value, whether from a reference material, a proficiency-testing target, or a comparison method. You estimate the bias with a confidence interval and test it against your allowable bias. An equality test asks whether bias is present. An equivalence test asks whether any bias is small enough not to matter clinically. Running precision and trueness together in one study is the efficiency EP15 was designed to deliver.

Troubleshooting a failed verification

A failed verification is a result to investigate, not a study to write off. Do not set it aside without investigating. Work through the likely causes before you accept or reject the method.

First, check for an outlier the ESD screen may have missed and a procedural cause: an operator unfamiliar with the assay, a reagent lot issue, an instrument not fully settled. A single bad day can fail a five-day study.

Second, consider whether the claim itself is stated under conditions you have not reproduced. A claim established over many days may legitimately exceed what five days captures. EP15 allows for that in the verification limit.

Third, if the imprecision is clear and repeatable and worse than claimed, that is a real finding. Escalate to the manufacturer with your data rather than absorbing it.

What you should not do is widen your goal after the fact to make a failure pass. The verification limit exists so that decision is made on the statistics, not on hope.

Downloads

Download the CLSI EP15-A3 verification example workbook (.xlsx) — a ferritin precision and trueness verification worked against a manufacturer’s claim, with χ² testing and generalised ESD outlier screening, ready to open in the Analyse-it trial.

Common mistakes

Running EP05 when EP15 would do. Establishing precision from scratch to bring a documented assay online is effort in the wrong place. Verify unless you specifically need to establish.

Verifying a modified or laboratory-developed test. The more dangerous error. If the manufacturer’s claims do not apply to your use, a short verification confirms nothing meaningful. You owe a full establishment.

Deciding after collecting data. Establishment and verification have different designs and sample sizes. Settle which you are doing before the first run, not after.

Comparing observed SD to the claim by eye. “Ours is a bit higher, close enough” is not a decision rule. Use the upper verification limit. The limit tells you whether the difference exceeds the sampling noise a small study inevitably carries.

Skipping the outlier screen. One aberrant replicate can fail a verification that the method would otherwise pass. Run the ESD screen before you judge the result.

Verifying precision but forgetting trueness. EP15 covers both in one study. Confirming imprecision while leaving bias unexamined answers only half the question the method needs to satisfy.

Relaxing the limit after a failure. Relaxing the allowable imprecision to convert a fail into a pass defeats the purpose of verifying at all. Investigate the cause instead.

Verify a precision claim with Analyse-it

Analyse-it runs the EP15-A3 verification on your own data, inside Excel:

  • Repeatability and within-laboratory precision, with χ² testing against the manufacturer’s claim
  • Bias, with both equality and equivalence tests
  • Generalised ESD outlier screening before either of them

Every feature from all five editions for 15 days. Precision and trueness verification is in the Method Validation and Ultimate editions, from US$ 475 a year. Validated against NIST and CLSI reference datasets. Full detail in the precision reference guide.